17th International Conference on Fundamental and Applied Aspects of Physical Chemistry (Proceedings, Volume I) (2024) [G-01-P, pp. 249-252]
AUTHOR(S) / АУТОР(И): S. S. Konstantinović, J. Savić and Dragan Z. Troter 
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DOI: 10.46793/Phys.Chem24I.249K
ABSTRACT / САЖЕТАК:
Synthesis of vanillin-thiosemicarbazone was performed by „greener“ one-pot batch technological procedure in ethanolic solution of citric acid under extremely mild operating conditions (20 °C and 10 min). The obtained compound was identified by elemental microanalysis, as well as FTIR and UV/Vis spectroscopic methods. Since ethanolic solution of citric acid behaved both as catalyst and solvent, the reaction was performed without any additional acidic catalyst. Compared to the conventional H2SO4-catalyzed synthesis in ethanol, the reaction time was shorter and the yield of obtained compound was higher.
KEYWORDS / КЉУЧНЕ РЕЧИ:
ACKNOWLEDGEMENT / ПРОЈЕКАТ:
This work was supported by the Republic of Serbia – Ministry of Science, Technological Development and Innovation (Programs for financing scientific research: 451-03-65/2024- 03/200133 and 451-03-66/2024-03/200133 assigned to the University of Niš, Faculty of Technology, Leskovac).
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