АУТОР(И): Milica Mačkić, Vojislava Bursić, Gorica Vuković, Tijana Stojanović, Dušan Marinković, Aleksandra Petrović, Nikola Puvača, Snežana Tanasković
In order to carry out the multi-residue determination of the pesticides in the soil the liquid chromatography coupled with tandem mass spectrometry with a triple quadrupole analyzer was applied. The basis of the method is the modified version of the environmentally friendly QuEChERS extraction. The validation parameters (linearity, recovery, precision, matrix effects, limit of detection and limit of quantification) were set in accordance with the SANTE/12682/2019. The obtained results show that the applied method represents the safe and reliable determination method for the cyprodinil, fenpropimorph, prochloraz and tebuconazole residues in the soil.
validation, soil, pesticide residues, LC-MS/MS
- Balkan T. (2021). Determination of chlorsulfuron and pendimethalin residues in soil using modified QuEChERS method by liquid chromatography tandem mass spectrometry. European Journal of Science and Technology No. 31 (Supp. 1), 539.
- Baloš M., Bursić V., Vuković G., Đurović-Pejčev R., Stojanović T., Petrović A., Marinković D., Špirović Trifunović B., Konstantinović B. (2020). Comparison of phenylurea pesticides recovery from different soil types, 26th International Symposium on Analytical and Environmental Problems, Syeged, Hungary, 88.
- Đurović-Pejčev R., V. Bursić, Zeremski T. (2019). Comparison of QuEChERS with traditional sample preparation methods in the determination of multiclass pesticides in soil. Journal of AOAC International, 102, 46.
- SANTE. (2019). Document No Sante/12682/2019 Method validation & quality control procedures for pesticide residues analysis in food & feed. European Commission: Brussels, Belgium.
- Sarkar S., Berbardes D.J., Keely J., Möhring N., Jansen K. (2021). The use of pesticides in developing countries and their impact on health and the right to food. EU publications. https://doi.org/10.2861/28995
- Vuković G., Vatazević A., Bursić V., Stojanović T., Petrović A., Marinković D., Špirović Trifunović B. (2021). Development and validation of a reable LC-MS/MS method for the nicotine residues determination in mushrooms, Journal of Agronomy, Technology and Engineering Management, 14(5), 635.